| Number of reaction vessels |
6 (3 with pre-activation option), no resin loader required |
| Synthesis scale range |
0.005 - 1 mmol per reaction vessel, (6 mmol in total)
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| Reaction vessel volume |
Plastic, disposable:10 mL, 45 mL Borosilicate glass:10 mL, 25 mL, 40 mL
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Number of solvent positions/sizes
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7 pressurized solvents (0.5 to 8 L vessels as standard, larger capacity vessels available)
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Number of amino acid positions
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27 amino acid bottles plus six Single-Shot only positions for specialty reagents.
10 mL (for standard or Single-Shot delivery for specialty reagents),120 mL, and 400 mL sizes.
Pre-packaged and empty bottles available.
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Chemistries supported
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Fmoc, t-Boc, organic, peptoid, combinatorial, branched, PNA
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Activation
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HBTU, HATU, HCTU, TBTU, PyBOP, DIC/OxymaPure, DIC/HOBt, others
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Throughput
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Fluid measurement technique
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Selectable fixed loop measurement with optical sensors for amino acids and reagents, timed delivery of solvents
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Fluid transfer method
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Positive pressure with nitrogen Top-down washing
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Agitation method
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Nitrogen bubbling - adjustable, and or optional Oscillation mixing - adjustable
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Cleavage
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Automated on-board cleavage, separate fluid path and vent
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Waste container
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(1) 20 L D.O.T rated container with over-flow sensor in cap
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Control interface
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Proprietary Prelude X control software, internal CPU, external keyboard, mouse, flat panel monitor
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Reporting
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Real-time log of each instrument function, print to file or printer.
Printable .pdf file for each method created. |
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Personalized user databases
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Individual users can create their own programs, peptide sequences, and syntheses that can only be accessed from their own personalized user database. Individual databases can be stored on the instrument, or on a portable USB drive.
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Start-up kit
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40 pre-packed AA bottles (20 natural amino acids; 5 mmol and 20 mmol scales), Reaction Vessels (Prelude disposable RVs, 30 pack of 10 mL and 30 pack of 45 mL RVs), Coated Glass RVs 6 pack each of 10 mL and 40 mL only for induction heat enabled instruments), Rink Amide Resin (0.1 mmol scale), Fmoc-Gly Wang Resin (0.1 mmol scale), HCTU (100 g), Activator Sample kit (5g each of K-Oxyma, PyOxim, OxymaPure and HDMA). Shipments to the USA also include 20% Piperidine/DMF and 0.4M N-Methylmorpholine/DMF (0.9 L each) reagents. (Cat#: PPX-STARTKIT/PPX-STARTKIT-I)
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Power
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115 V/60 Hz or 230 V/50 Hz
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Dimensions (W x D x H)
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34.5” x 28” x 36.25” (87.6 cm x 71 cm x 92 cm)
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Approximately 260 lbs. (118 kg)
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One year, parts and labor.
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OPTIONAL - Heating and mixing
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Six individually controlled induction heating units (Cat#: PPX-IHEAT-OPT) Adjustable oscillating mixing unit (Cat#: PPX-SHAKE-OPT) software and heating control systems
Intellisynth Real-time UV Monitoring and feedback control system and software (Cat#: PPX-UV-OPT). Learn more
Preset Prelude X to ensure your synthesis is protected. The Safe Response software feature can be setup to rinse and drain a reaction with a solvent of your choosing if a synthesis is interrupted for any reason. Dynamic Sequence Programming option allows the reaction vessels to operate semi-independently. Have one peptide run a special cycle in the middle of a sequence while the other reaction vessels sit idle. Add pre- or post-processing cycles. (Cat#: PPX-DYN-SEQ-PGM) E-mail-Text Message Status Reporting. Always be “in touch” with your synthesis and have Prelude X send an email to a computer or cell phone at a specified program step, at the beginning of each cycle, or if an error occurs. (Cat#: PPX-TXT-EML-RPT). Learn morePre-activation Programming (Cat#: PPX-PRE-ACT-PGM)
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